Web(A) Total ion chromatography of HILIC-FTMS profiling of fully digested KS domain structure. (B) Composition analysis of KSO calculated by GlycResoft. The analytical error for each … WebNov 7, 2016 · The HILIC-FTMS method was developed using mixed standards of polar metabolites and lipids, the separation efficiency of which is better in HILIC mode than in …
HILIC-MS for metabolomics: An attractive and complementary
Web2.1. HILIC–ESI-FTMS Analysis of Phospholipids in Fresh Seafood Products. By analogy with previous investigations on mussel phospholipids [17,18,19], HILIC–ESI(+)-FTMS was adopted for the initial characterization of the main PL classes in the seafood products of interest, which were all examined as fresh products in the first step of the study.As … WebJul 1, 2024 · Two-dimensional NMR spectroscopy and HILIC-FTMS were performed to investigate the structural characteristic of FCS hf. RAW 264.7 cells were exposed to FCS hf at different concentrations to evaluate its proliferation, NO production and … famous birthdays feb 1
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WebDec 12, 2016 · Online hydrophilic interaction chromatography (HILIC) Fourier transform mass spectrometry (FTMS) was performed as previous described [ 4 ]. Briefly, enoxaparin injections were diluted into 1 μg/μL and directly injected into a HILIC column (2.0 mm × 150 mm, 200 Å, Phenomenex, Torrance, CA) by an Agilent 1200 autosampler. WebJun 15, 2024 · Oligosaccharides profiling of FCS sj by HILIC-FTMS FCS sj was degraded by controlled peroxide oxidation using hydrogen peroxide and ascorbic acid (Li et al., 2024 ). In brief, FCS sj (1 mg) was dissolved in 600 μL of 100 mM H 2 O 2 containing 48 mM ascorbic acid, and incubated at 45 °C for 3 h. WebApr 1, 2024 · HILIC-FTMS analysis Free-radical degraded oligosaccharides were analyzed using HILIC-FTMS, which was performed on an Agilent 1290 LC UPLC system (Agilent Technologies, Wilmington, DE, USA) equipped with an LTQ ORBITRAP XL mass spectrometer (Thermo Fisher Scientific, Waltham, MA, USA). co op testing